Sunday January 22nd, 2017 14:25 Dry ice extraction experiment and a possessed test tube

This video is just a experiement me and my friends did for our Analytical Chem experiment at Kwantlen Polytechnic Uinversity. What I wanted to show was some of the stuff that happens in a chem lab to people or students who havn’t seen stuff in a lab before. In the first part of the video, i want to show what happens when you drop a piece of dry ice in a beaker full of hot water. As everyone can see, it immediatly sublimes. In the second part of the video, we are performing the experiement for that day. We are extracting Limonene oil from Orange rinds( orange zest for thoughs cooks out there). First, we fill a tube with a copper mesh on the bottom half with the rind and the rest with compacted, crushed dry ice. The sealed tube is placed in the hot water so that the ice can begin to sublime. As the pressure builds, the ice can no longer sublime anymore. Instead, the pressure causes the ice to melt in to liquid carbon dioxide, and boil on contact with the rinds. Almost like liquid nitrogen, but warmer. As the liquid goes through the rinds, it picks up the oil, and anyother oils in the rinds, and brings them down to the bottom of the tube. This is a similar technique some companies use to decaff coffee with out using harmful solvents. Just as a note, there is no mixer in the graduated cylinder, the tube is spinning on its own This video was shot with my blackberry, so i know that the video quality is crappy and the audio isnt very good.

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    376 Comments on “Dry ice extraction experiment and a possessed test tube”

    • threejchapman May 11, 2011 at 5:57 am

      what kind of test tube is that? can you tell me a online page to order them from?
      do you think that I could get the same reaction on a larger scale if I use a pressure cooker with a regulator on it that would kick in at 80 psi.

    • mythrhun May 12, 2011 at 12:38 pm

      It’s a Centrifudge Tube

    • wazscience May 13, 2011 at 6:12 am

      @threejchapman the tube that we used was a 50 ml conical centrifuge tube. we used this tube because when we would insert the copper wire mesh to hold back the rinds, the mesh would stop at the base of the cone leaving a small space to collect the oil. im not sure what site you could go to inorder to obtain tubes since i got the tubes from my school lab. I guess you could do this in a larger scale. You would need an apparatus that would allow you to pour the liquefied co2 over a material.

    • wazscience May 13, 2011 at 6:16 am

      @threejchapman and collect the extracted oils all in the same container.

    • wazscience May 25, 2011 at 2:52 am

      wow… this video almost has as many view as my channel does

    • meyepen June 13, 2011 at 10:33 pm

      How do you get ALL the limonene out of the bottom of the test tube?

    • guninhatersdown June 15, 2011 at 9:57 am

      scientific glass is no more fun without being able to smoke out of it

    • robertomasymas July 2, 2011 at 8:07 am

      how much pressure can dry ice melting generate?

    • wazscience July 2, 2011 at 9:49 am

      @robertomasymas a fair amount. Dry ice normally likes to sublime due to the huge temperature diffrence between the ice and environment. In order to form liquid carbon dioxide, liquid dry ice, requires a high enough pressure to force the atoms of the gas close enough to form a liquid. I cant really give you a close enough range to what the pressure would be, but all i cant say it that the tube is like a mini co2 canister.

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